Analytical methods

ExperimentID EXA000611
ChemicalID CH0000926
Chemical Name Carbon disulfide
Official Method No
Chromatography Head space GC
Chromatography mfr. 7890A, Agilent equipped with Head space: 7697A, Agilent
Column InertCap AQUATIC 60 m x 0.25 mm, 1.0 μm
Column mfr. GL Sciences
Detector MS
Detector mfr. 5975C, Agilent
Ionization SIM-EI
Extraction
Extraction Details
Clean-up 1st Salting out
Clean-up 1st Details Sodium chloride
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike
Syringe Spike Fluorobenzene; p-bromofluorobenzene
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 4.2 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf
Remarks Analysis method: p.4
RegisterDate 2022/11/25
UpdateDate 2022/11/25