| ExperimentID |
EXA000612 |
| ChemicalID |
CH0001399
|
| Chemical Name |
Dimethyl phthalate |
| Official Method |
No |
| Chromatography |
GC; GSMS |
| Chromatography mfr. |
[1]7890A, Agilent; [2]GCMS-QP2020, Shimadzu |
| Column |
J&W DB-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
[1]5975C, Agilent |
| Ionization |
SIM-EI |
| Extraction |
SPE |
| Extraction Details |
Oasis HLB Plus; Eluted with Acetone |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
Dimethyl phthalate-d4 |
| Syringe Spike |
Phenanthrene-d10 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
11 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.5 |
| RegisterDate |
2022/11/25 |
| UpdateDate |
2022/11/25 |
