Analytical methods

ExperimentID EXA000612
ChemicalID CH0001399
Chemical Name Dimethyl phthalate
Official Method No
Chromatography GC; GSMS
Chromatography mfr. [1]7890A, Agilent; [2]GCMS-QP2020, Shimadzu
Column J&W DB-5ms 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector MS
Detector mfr. [1]5975C, Agilent
Ionization SIM-EI
Extraction SPE
Extraction Details Oasis HLB Plus; Eluted with Acetone
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Dimethyl phthalate-d4
Syringe Spike Phenanthrene-d10
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 11 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf
Remarks Analysis method: p.5
RegisterDate 2022/11/25
UpdateDate 2022/11/25