Analytical methods

ExperimentID EXA000615
ChemicalID CH0001400
Chemical Name Di-n-butyl phthalate
Official Method No
Chromatography GC
Chromatography mfr. 7890A, Agilent
Column InertCap 1MS 30 m x 0.25 mm, 0.25 μm
Column mfr. GL Sciences
Detector MS
Detector mfr. 5975C, Agilent
Ionization SIM-EI
Extraction Solvent Extraction
Extraction Details Extracted with Hexane; Shaken for 5 min.
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike Di-n-butyl phthalate-d4
Syringe Spike p-Terphenyl-d14
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 18 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf
Remarks Analysis method: p.5
RegisterDate 2022/11/25
UpdateDate 2022/11/25