Analytical methods

ExperimentID EXA000623
ChemicalID CH0001042
Chemical Name 2-sec-Butylphenyl N-methylcarbamate (synonym: Fenobucarb or BPMC)
Official Method No
Chromatography LC
Chromatography mfr. ExionLC, AB Sciex
Column L-column ODS 150 mm x 2.1 mm, 5 μm
Column mfr. CERI
Detector MS/MS
Detector mfr. QTRAP 6500QT, AB Sciex
Ionization SRM-ESI-positive
Extraction SPE
Extraction Details
Clean-up 1st Washing
Clean-up 1st Details Washed in purified water
Clean-up 2nd Filtration
Clean-up 2nd Details Filtered with 13 mm GD/X syringe filter, PVDF 0.2 μm, Whatman
Clean-up Spike
Syringe Spike Diuron-d6
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 0.052 ng/L
Method Quantification Limit
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf
Remarks Analysis method: p.6
RegisterDate 2022/11/25
UpdateDate 2022/11/25