| ExperimentID |
EXA000623 |
| ChemicalID |
CH0001042
|
| Chemical Name |
2-sec-Butylphenyl N-methylcarbamate (synonym: Fenobucarb or BPMC) |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
ExionLC, AB Sciex |
| Column |
L-column ODS 150 mm x 2.1 mm, 5 μm |
| Column mfr. |
CERI |
| Detector |
MS/MS |
| Detector mfr. |
QTRAP 6500QT, AB Sciex |
| Ionization |
SRM-ESI-positive |
| Extraction |
SPE |
| Extraction Details |
|
| Clean-up 1st |
Washing |
| Clean-up 1st Details |
Washed in purified water |
| Clean-up 2nd |
Filtration |
| Clean-up 2nd Details |
Filtered with 13 mm GD/X syringe filter, PVDF 0.2 μm, Whatman |
| Clean-up Spike |
|
| Syringe Spike |
Diuron-d6 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.052 ng/L |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_2_2.pdf |
| Remarks |
Analysis method: p.6 |
| RegisterDate |
2022/11/25 |
| UpdateDate |
2022/11/25 |
