Analytical methods

ExperimentID EXA000750
ChemicalID CH0000365
Chemical Name PFOS
Official Method No
Chromatography LC
Chromatography mfr. ACQUITY UPLC I-Class, Waters
Column BEH C18 50 mm x 2.1 mm, 1.7 μm
Column mfr. Waters
Detector MS/MS
Detector mfr. API-6500, AB Sciex
Ionization SRM-ESI-negative
Extraction SPE
Extraction Details pH adjustment: pH 6.0-11; SPE:(Front stage) Presep-C Alumina, (Second stage) Presep-C Agri; Eluted with Methanol
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 13C4PFOS
Syringe Spike
Derivatization
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 30 pg/L
Method Quantification Limit 80 pg/L
Repeatability
Standard
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Protocol https://www.env.go.jp/chemi/kurohon/2021/shosai/5_3_2.pdf
Remarks Analysis method: p.8
RegisterDate 2023/1/26
UpdateDate 2023/1/26