| ExperimentID |
EXA000753 |
| ChemicalID |
CH0001174
|
| Chemical Name |
Hexachloro-1,3-butadiene |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
7890, Agilent |
| Column |
DB-5ms 30 m x 0.25 mm, 0.25 μm |
| Column mfr. |
Agilent |
| Detector |
MS/MS |
| Detector mfr. |
7010, Agilent |
| Ionization |
MRM-EI |
| Extraction |
Reflux extraction |
| Extraction Details |
Extracted with Hexane; Reflux boiling for 60 min.; Dehydration with Whatman 1PS filter |
| Clean-up 1st |
|
| Clean-up 1st Details |
|
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
13C4-Hexachloro-1,3-butadiene |
| Syringe Spike |
Naphthalene-d8; Acenaphtene-d10; Phenanthrene-d10; Fluoranthene-d10; Chrysene-d12 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
40 pg/L |
| Method Quantification Limit |
100 pg/L |
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
https://www.env.go.jp/chemi/kurohon/2021/shosai/5_3_2.pdf |
| Remarks |
Analysis method: p.9 |
| RegisterDate |
2023/1/26 |
| UpdateDate |
2023/1/26 |
