Analytical methods

ExperimentID EXA000797
ChemicalID CH0001174
Chemical Name Hexachloro-1,3-butadiene
Official Method No
Chromatography GC
Chromatography mfr. 7890, Agilent
Column DB-5ms 30 m x 0.25 mm, 0.25 μm
Column mfr. Agilent
Detector MS/MS
Detector mfr. 7010, Agilent
Ionization MRM-EI
Extraction Reflux extraction
Extraction Details Extracted with Hexane; Reflux boiling for 60 min.; Dehydration with Whatman 1PS filter
Clean-up 1st
Clean-up 1st Details
Clean-up 2nd
Clean-up 2nd Details
Clean-up Spike 13C4-Hexachloro-1,3-butadiene
Syringe Spike Naphthalene-d8; Acenaphtene-d10; Phenanthrene-d10; Fluoranthene-d10; Chrysene-d12
Recovery Correction
Instrument Detection Limit
Instrument Quantification Limit
Method Detection Limit 10 pg/g dry
Method Quantification Limit 30 pg/g dry
Recovery (CRM)
Recovery (spiked)
Recovery (IS)
Remarks Analysis method: p.10
RegisterDate 2023/2/15
UpdateDate 2023/2/15