| ExperimentID |
EXA000857 |
| ChemicalID |
CH0001644
|
| Chemical Name |
TCIPP |
| Official Method |
No |
| Chromatography |
LC |
| Chromatography mfr. |
Prominence UFLC XR, Shimadzu |
| Column |
Ascentis Express C18 analytical column (2.7 |
| Column mfr. |
Supelco |
| Detector |
MS/MS |
| Detector mfr. |
AB SCIEX QTRAP 5509 mass spectrometer, Sciex |
| Ionization |
ESI |
| Extraction |
Ultrasonic Extraction |
| Extraction Details |
Extracted with a mixture of dichloromethane/n-hexane (1:1 v/v, 9 mL) |
| Clean-up 1st |
SPE |
| Clean-up 1st Details |
Supelclean ENVI-Carb II/PSA SPE cartridge |
| Clean-up 2nd |
|
| Clean-up 2nd Details |
|
| Clean-up Spike |
d15-TEP; d27-TNBP; d21-TPP; d15-TPHP; d21-p-TMPP; d12-TCEP; d15-TDCIPP |
| Syringe Spike |
|
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
657 fg |
| Instrument Quantification Limit |
|
| Method Detection Limit |
0.39 ng/g ww |
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
1970/1/01 |
| UpdateDate |
1970/1/01 |
