| ExperimentID |
EXA000898 |
| ChemicalID |
CH0000074
|
| Chemical Name |
PCB167 |
| Official Method |
No |
| Chromatography |
GC |
| Chromatography mfr. |
7890A, Agilent |
| Column |
DB-1MS column (30 m x 0.25 mm x 0.25 |
| Column mfr. |
Agilent |
| Detector |
MS |
| Detector mfr. |
5975C, Agilent |
| Ionization |
EI |
| Extraction |
ASE |
| Extraction Details |
Extracted with a mixture of acetone and n-hexane (1:1, v/v) |
| Clean-up 1st |
GPC |
| Clean-up 1st Details |
|
| Clean-up 2nd |
Activated silicagel column |
| Clean-up 2nd Details |
|
| Clean-up Spike |
13C12-PCB28; 13C12-PCB52; 13C12-PCB95; 13C12-PCB101; 13C12-PCB105; 13C12-PCB118; 13C12-PCB138; 13C12-PCB153; 13C12-PCB156; 13C12-PCB157; 13C12-PCB167; 13C12-PCB178; 13C12-PCB180; 13C12-PCB189; 13C12-PCB194; 13C12-PCB202; 13C12-PCB206; 13C12-PCB208; 13C12-PCB209 |
| Syringe Spike |
13C12-PCB170 |
| Derivatization |
|
| Recovery Correction |
|
| Instrument Detection Limit |
|
| Instrument Quantification Limit |
|
| Method Detection Limit |
|
| Method Quantification Limit |
|
| Repeatability |
|
| Standard |
|
| Recovery (CRM) |
|
| Recovery (spiked) |
|
| Recovery (IS) |
|
| Protocol |
|
| Remarks |
|
| RegisterDate |
1970/1/01 |
| UpdateDate |
1970/1/01 |
